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A. INTRODUCTION :
A.1
Calibration data for:
Calibration constants:
| SQUIDS: |
|
| X axis = |
10-5 emu/ flux quanta |
| |
div. DC offset per flux quanta |
| |
div. DC bias |
| Y axis = |
10-5 emu/ flux quanta |
| |
div. DC offset per flux quanta |
| |
div. DC bias |
| Z axis = |
10-5 emu/ flux quanta |
| |
div. DC offset per flux quanta |
| |
div. DC bias |
FIELD CONTROL COILS:
Sense region trim coils:
These coils are helmholtz pairs of 15 turns
each coil of 0.016 inch insulated copper wire wrapped directly
on the 21 inch OD dewar vacuum jacket.
The Axial trim coil: 1 milliamp =
60 gamma
The SQUID direction trim coil: 1 milliamp
= 70 gamma
The Fill port direction trim coil: 1 milliamp
= 70 gamma
TEMPERATURE SENSORS:
The equilibrium diode voltages at temperatures
shown are:
| diode location |
BNC |
box |
295K |
77K |
65K |
15K |
4.3K |
| shield |
T1 |
1 or 2 |
|
0.4 |
1.0 |
1.05 |
N/A |
| reservoir |
T2 |
1 or 2 |
|
0.4 |
1.0 |
1.05 |
N/A |
| cryocooler - inner |
T1 |
3 |
0.4 |
1.0 |
1.05 |
|
N/A |
| cryocooler - outer |
T2 |
3 |
0.4 |
1.0 |
1.05 |
N/A |
N/A |
(N/A = not applicable.)
FLOW GAUGE CALIBRATION:
The floating ball flow gauge was calibrated
against an absolute displacement gauge at three points as
given below:
Flow gauge reading boil
off
20 cc/m
0.07 liter per day
30 cc/m
0.10 liter per day
40 cc/m
0.15 liter per day
A.2. SUMMARY TRANSFER PROCEDURE
- SRM DEWAR
1. Preparation : Collect all equipment near the SRM dewar
(SRM).
Supply dewar (SUPPLY).
Helium gas supply
Heat Gun
Transfer line (LINE).
Transfer adapter (ADAPTER) with stoppers and clamps.
Record all health parameters (2-1-c). Numbers in (--) refer
to detailed procedures. 4 temperatures, SQUID bias levels,
safety pressure, cryocooler pressure
2. Bleed the pressure in the SUPPLY to atmospheric pressure
(2-1-f) and measure liquid level.
3. Bleed the SRM to 2 psig (2-1-g). Close the needle valve
at popoff valve from vent damper (2-1-h).
4. Attach the ADAPTER to the SRM side of the transfer LINE.
Adjust clamps to snug fit on LINE
§ (2-1-i).
5. Thoroughly flush LINE with helium gas (about 1 minute)
, holding as an inverted "U", and make certain that
the closed end extension is attached to SUPPLY side of line.
Slowly insert the LINE into the SUPPLY (2-2-c), keep SUPPLY
vent open and at one atmosphere.
6. Apply about 1/4 psig helium gas pressure to SUPPLY to
get a small flow of gas out of the LINE. Open flip valve on
ADAPTER. While exit gas is still warm quickly insert
the LINE with ADAPTER into fill port. Tighten the hose clamp
around the fill port and gently push LINE into fill
port until it bottoms, then pull out 1/2 inch.(2-2-c).
7. Increase the transfer (SUPPLY) pressure to 2 psig (2-2-c).
8. When this exhaust gas get cold and ADAPTER is beginning
to frost, close the flip valve (2-2-c) NOTE: the gauge
on ADAPTER will oscillate by about +/- 1 psig when LINE is
precooled. Push LINE to seat in fill port. Tighten hose
clamp, ADAPTER to LINE, so no gas leaks.
9. Slowly increase the transfer pressure to 3 psig, monitoring
the SRM safety pressure. When the SAFETY pressure reaches
about 2 psig FULLY open the SRM vent valve (2-2-d). Turn vent
valve back and forth when opened until it is cold, to help
prevent valve stem seal from freezing.
10. THIS IS THE MOST CRITICAL TIME OF THE TRANSFER- EXTREME
CAUTION MUST BE USED TO PREVENT BACK DRAFTING OF AIR INTO
THE SRM VENT PORT (10-2-e).
11. If the safety pressure falls below 1 psig the VENT valve
must be closed. Seal vent with red stopper & heat VALVE
if necessary to close. Continue the transfer without changing
transfer pressure, with the VENT valve closed. Hold the transfer
pressure constant until safety pressure rises to 2 psig ,
open the vent valve (2-2-f).
12. Maintain the transfer pressure at 3 psig CONTINUOUSLY
MONITORING THE SAFETY PRESSURE. If the safety pressure falls
again to below 1 psig the vent valve must be closed again
, then repeat step 11, (2-2-e).
13. Hold the transfer pressure constant and read the helium
level gauge every minute - the level should increase at about
5 percent per minute (2-2-g).
14. When the SRM is full or the SUPPLY is empty the SAFETY
pressure will abruptly rise about one psig. Also, the level
gauge readings will stop increasing. At this time stop the
transfer by opening the vent valve on the SUPPLY and start
venting to one atmosphere (2-2-i). Leave the SRM VENT valve
open at this time.
15. As soon as the SAFETY pressure falls to 2 psig close
the VENT valve on the SRM (2-2-j).
16 The transfer may be continued from a second SUPPLY or
it may be stopped.
17 To continue from a second SUPPLY, remove the transfer
line and adapter from the SRM fill port and immediately plug
the fill port (2-3-b). Now remove the LINE from the
depressurized SUPPLY and warm the inside of the line to room
temperature by flowing helium gas thru the line. Do not try
to conserve helium by starting the next transfer with the
cold line, the probability of getting air and/or moisture
into the fill port is much too great.
18 Follow steps 5 thru 14 above.
19 Additional SUPPLY dewars may be used as necessary.
20 Termination of the transfer from step 15 above, with the
SUPPLY at one atmosphere, the safety pressure at 2 psig ,
and the LINE still in the SUPPLY and SRM
21 Loosen the hose clamp on the ADAPTER to FILL port and
quickly remove the LINE and ADAPTER from the fill
port. Plug the port immediately with the black rubber
stopper (2-3-b).
22 Warm the FILL and VENT ports with a heat gun then remove
the stopper from the FILL port and fit the brass cap with
its pop off.
23 Check to make certain that the SRM vent valve
is warm and closed. Open the valve at the flow gauge Pop-off
valve. All vent gas will now flow through this pop-off
valve and the flow gauge (2-5-b).
24 Remove the transfer line from the SUPPLY and close its
transfer port (2-4-a). Measure the helium left in the
SUPPLY and the final level in the SRM and record.
A.2. Suggested data recording for 755 and
760 2G magnetometers
DAILY:
1. Gas flow gauge. Should be between 0 and 40 divisions.
2. Pressure on safety gauge. Should be about 2.0 psig.(2/15
bar).
3. Atmospheric pressure, if convenient.
4. Measure and record standard sample. Dipole moment to be
about
1 X E-5 emu on each axis.
5. Wipe sample handler bars with clean cloth and use light
spray of dry silicone or teflon lubricant.
WEEKLY:
1. SQUID signals with scope. Record peak to peak AC voltage,
and value of I BIAS potentiometer.
2. Liquid helium level gauges, #1 and #2.
Should decrease about 2 % on one gauge per week. Each
gaugemeasures 50% of the total liquid volume, unless the system
has a single level gauge sensor.
3. Temperatures T1 and T2 using boxes #2 and #3. DO NOT USE
BOX #1 except for heating the shield, SQUIDS or pickup coils.
4. Cryocooler compressor pressure. This should be about 270/280,
and should fluctuate by about 5 psig each cycle..
EACH YEAR:
Change the cryocooler adsorber. This takes about 30 minutes
and is done with the magnetometer cold. New adsorbers are
available through directly from CTI new adsorbers cost about
US$550. Please refer to the CTI manual for addresses.
SYSTEM EVACUATION AND COOL DOWN:
The system is normally pumped
out and cooled to liquid helium temperatures prior to delivery
and whenever possible we deliver systems filled with liquid
helium. This section of the manual is provided in the event
that the system needs to be warmed to room temperature for
any reason and then the customer needs to check the vacuum
and conduct the complete cool down. In the following discussion,
we assume that the SRM (Superconducting Rock Magnetometer)
is at room temperature and under vacuum.
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